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  1. Rabidreject

    Looking to do a Henry reduction on 3,4,5-trimethoxybza…

    I mean, the synth I was looking at on here said cyclohexalymine - I do have a big bottle of cyclohexanone as well. Was thinking of doing the rxn with ammonia but the synth I’m reading used Zn powder - could I use something else? I am assuming all we are doing here is reductive amination? I say all…
  2. Rabidreject

    Looking to do a Henry reduction on 3,4,5-trimethoxybza…

    I can easily get cyclohexylamine hydrobromide, would this work?
  3. Rabidreject

    Looking to do a Henry reduction on 3,4,5-trimethoxybza…

    Hi guys, I’m looking to make some mescaline, I have everything under control in terms of acquisition of chems apart from, the cyclohexylamine. I had issues with the n-butylamine before which is why I havnt used my nitroethane for amphetamine at all. dang primary amines… Could this be switched...
  4. Rabidreject

    Small batch chemist looking to do the Henry reaction….

    Yeah I’m not suggesting I turn my benzaldehyde into anything else, either someone please sell me some n-butylamine or let me know if methylamine would work as I could potentially make a small amount. (Obviously with other materials) I was really hoping someone would say yeh I’ll sell you 250g...
  5. Rabidreject

    Small batch chemist looking to do the Henry reaction….

    Hi guys, I’m curious if anyone on here would sell me relatively small amounts of a few different aldehydes so that with the help of both nitromethane and nitroethane I can explore the worlds of psychedelic amphetamines and PEA’s, without having to buy each different aldehyde in 500g quantities...
  6. Rabidreject

    Hoping this is the correct place to ask about TLC?

    No I don’t mean the plates regarding the ‘wick’ - on the diagram I looked at they had the stationary phase (the silica plates) and the mobile phase (the solvent or mix of) which they then put into a tub and used a ‘wick’ behind the plate but not touching for the solvent to travel up and turn...
  7. Rabidreject

    1-nitropropane

    Hi guys, I have a product that contains 1-nitropropane and nitroethane along with DCM. My chemist friend seemed more excited about the nitropropane but im confused as iv never seen it used in synths for phenethylamines (which is what im primarily interested in - as is my friend) Any ideas? Is...
  8. Rabidreject

    MDP2P From PMK Glycidate

    Oh also, I mean for the final step once you have your MDP2P for the reductive amination….obviously haha I dunno why I felt I had to clarify that to a room full of chemists!
  9. Rabidreject

    MDP2P From PMK Glycidate

    Oh and as for freeze point can’t you simply lookup the freezing point of MDP-2-P? Or is it the glycidate you are talking about freezing?
  10. Rabidreject

    MDP2P From PMK Glycidate

    My other question still stands though, can you get away with using NaBH4 instead of something like LiAlH4
  11. Rabidreject

    MDP2P From PMK Glycidate

    Oooh okay so you to perform an acid/base reaction by the look of things…my bad
  12. Rabidreject

    MDP2P From PMK Glycidate

    My understanding, and I was just about to ask about this, is that you have to react it with an acid (I read HCL but can’t remember what strength - think it was 35%) and then proceed with the PMK. I need to do some reading on the area but my understanding was that after that you just need to do...
  13. Rabidreject

    Polish nitroethane/nitromethane

    Looking for a vendor 
    Sorry kingship, sincerely. This was out of order saying that. I was just confused by your answer and I’m doing a benzo detox at the mo. Very snappy - I really do appologise for such an arrogant answer…
  14. Rabidreject

    Polish nitroethane/nitromethane

    Looking for a vendor 
    I actually found a great product that’s sold in the UK and isn’t even an unusual product for me to order. I am an art student and there is an acrylic glue that is made of DCM and nitroethane. It just came and was expecting the methanol so I can get on with the DMT/DET syntheses but nope….lol i...
  15. Rabidreject

    Polish nitroethane/nitromethane

    Looking for a vendor 
    Dang - nitrochemis wont ship nitroethane to my country…how annoying. I’m getting this a lot with these substances - I’m guessing they can’t go on a freight plane… I guess I could buy some P2NP but that wasn’t really the point… Seems like every ‘source’ I come across doesn’t ship to the Uk. The...
  16. Rabidreject

    Polish nitroethane/nitromethane

    Looking for a vendor 
    What do you mean? There is nitro in the country? Yes there is, if you are either working at a registered business OR you have a link - which is what I am asking around for! Gosh, people are MUCH harder for me to deal with than chems. Appologies if I sound like a dick fumbling about but everyone...
  17. Rabidreject

    Polish nitroethane/nitromethane

    Looking for a vendor 
    Ah yeh I did look at nitrochemis actually - I just lost the link! Much appreciated for that! I know it’s in the links section but I must have missed it the second and third times I looked - I remember seeing P2NP on this site.
  18. Rabidreject

    Polish nitroethane/nitromethane

    Looking for a vendor 
    To be fair, it’s pretty easy to get shit posted to the UK. It’s been how iv received ALL my reagents and solvents so far. That website has changed my world…
  19. Rabidreject

    DMT and other tryptamine synth questions….please help…

    Just a simple water bath with timer and PID heated. It was $40 so I figured why not - it isn’t necessarily for this. I will have tried it a few times by the time that arrives, I’m aware of that. I also bought a vacuum aspirator while I was at it and some more boro stirring sticks - ***** I...
  20. Rabidreject

    DMT and other tryptamine synth questions….please help…

    Oh that’s fine, I have diethyl-ether anyway so that’s great, iv been waiting for a use for it lol
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