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  1. Rabidreject

    Does this actually make sense?

    Hi guys, I guess I have two questions I guess but they are both relating to the same subject - sodium ethyl sulfate. Okay so first things first - does this synthesis make sense? I know that mixing sulphuric acid and azeotropic 98% ethanol to make sulfonic acid and from there basically basify...
  2. Rabidreject

    Looking for a suitable, adjustable vacuum pump..

    By the way, thanks for replying to my post, I’m pretty new to posting on here and have been a long time lurker - ever since I found you at least! It has also lead (no pun intended) to me meeting at least 1 person who actually knows what they are doing and I find very inspiring….
  3. Rabidreject

    Looking for a suitable, adjustable vacuum pump..

    Funnily enough, I met a chemist on here and he said exactly the same thing. I also watched a video on pootube on it and that furthered my understanding. I have used a hand vacuum pump before but it broke. I ended up going with a pump that is basically two in one, positive pressure as well as...
  4. Rabidreject

    Is nitromethane useful for phenethylamines other than mescaline?

    That makes infinitely more sense - although I’d kind of gathered it by looking at the literature so much by now BUT I didn’t really understand WHY. So thanks for that!
  5. Rabidreject

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    Look at hydroponic ph+ solution - it is 35% I am from the UK. Dunno if that would suffice but those are how I get my hydrogen peroxide and my 35% sulphuric acid also tbf! Very useful for multiple applications in my life!
  6. Rabidreject

    Anyone here tried making 2,5-dimethoxybenzaldehyde using benzaldehyde and pyridine?

    Yeah I learnt. I realised like 5 mins after I posted this I meant something like 3,4-hydroxy ph or something, got confused between the mescaline precursor, the 2c main precursor and 3,4hydroxyphenrthylamine. Totally different …sorry about that. Iv since had a lesson on phenethylamines and the...
  7. Rabidreject

    Synthesis of 25B-NBOME from benzaldehydes with nitromethane

    Not yet, but I’m collecting the relevant compounds. I’m going to just do a reduction of P2NP first to r-amphetamine. Then, when I have a decent pump and a better non clogged Buchner. I want the pump for rxns as well though so I need it adjustable with a monitor and able to pull something like...
  8. Rabidreject

    Looking for a suitable, adjustable vacuum pump..

    So I’m looking for a vacuum pump that will reliably pull a vacuum of 640 mm hg. I’m totally new to vacuum distillation and am trying to make use of my benzaldehyde without having to get nitroethane as I can’t find it. I need a decent vacuum pump for a Buchner anyway - I’m not sure if they are...
  9. Rabidreject

    Have I FINALLY done it?

    I followed the write up on the rhodium archives that used the l-carvone in spearmint oil, only I swapped that out for cyclohexanone (from the ketone catalysed write up above). That was essentially it. I still have some of the ‘mother liquor’ so I may use it to see if I can decarb any more with...
  10. Rabidreject

    Have I FINALLY done it?

    So as I’m sure a few of you have gathered iv been trying the ketone catalysis of tryptophan to yield tryptamine but was having issues. turns out I just couldn’t follow instructions because I was taking breaks, not making notes and forgetting where I was. I’m pleased to say iv corrected these...
  11. Rabidreject

    Synthesis of 25B-NBOME from benzaldehydes with nitromethane

    You arnt talking to yourself at all. This is very interesting article to me and one I’m gathering my supplies to try. I love the idea of having such a powerful psychedelic! I’d never be irresponsible with it and try to pass it of as acid - that’s what ruined these drugs in my opinion. It...
  12. Rabidreject

    Anyone here tried making 2,5-dimethoxybenzaldehyde using benzaldehyde and pyridine?

    At least I could make mescaline in small quantities….
  13. Rabidreject

    Anyone here tried making 2,5-dimethoxybenzaldehyde using benzaldehyde and pyridine?

    Pretty much all in the title but if you have, can you give me an idea of how easy it is? I have a load of benzaldehyde and I’m not into amphetamine’s very much, I would much rather convert it to 2,5-dmobzh (yes that’s my shorthand for the above chem lol) and risk getting half the amount of...
  14. Rabidreject

    Is nitromethane useful for phenethylamines other than mescaline?

    Oh I also have benzene. Just normal benzene, I’m sure I could make P2NP but again don’t really want something that doesn’t make me trip.
  15. Rabidreject

    Is nitromethane useful for phenethylamines other than mescaline?

    I just ordered some nitromethane thinking I was going to make some substituted phenethylamines but it seems like the only synthesis I can do with it really that I would want to is to make mescaline etc…any ideas or anything I’m missing, I was hoping to be able to just buy 2,5-dmo benzaldehyde...
  16. Rabidreject

    Cannabidiol (CBD) Isomerization to Psychoactive Cannabinoids

    You should check out the book written by ‘Michael Valentine Smith’ a pseudonym of another well known psychedelic chemist and just a fantastic all round chemist, called Psychedelic chemistry. It was written, I believe, back in the 70’s. It has quite a bit about cannabis chemistry also…this stuff...
  17. Rabidreject

    Reduction of Tryptamine using STAB. Advice?

    Okay so I’m doing an aminative reduction of tryptamine to yield various different primary active tryptamines. I will be using the method that is on video, filmed by Hamilton Morris - not the one where HE makes MEO, the one with the weird third eye guy lol I’ll be making sodium...
  18. Rabidreject

    Top factories, precursor materials, safe transportation, raw material supply, contact information, technical support, stable supply

    Hey there fellow, I’m looking for comparatively small quantities of multiple substances. In particular I’m looking for around 100g of tryptamine, 50g-100g of 2,5-dimethoxy benzaldehyde. I’m not looking to supply the whole world or anyone other than friends so I don’t need Kilo’s and kilo’s. Are...
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