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May I have a question about the ma.HCI part ? I’ve watched your other post about adding ma.HCI directly into the mixture, and I also try it once recently, I have a problem when I dissolved the 2b4m in solvent, should I followed with NaOH + water and start stirring, then adding MA.HCI immediately with small portions? If I didn’t misunderstand it, the whole mixture would turn dark after adding NaOH water, it’s happening before any MA.HCI followed, because it was what happened during my synthesis, so am I did anything wrong ? Or it is normal ? Best regards
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Hi, I never try with ma HCl personnally but water turning black with naoh is not very surprising, try to add rge ma hcl not too slow tho, just avoid overheating. sorry for the late reply, I didn't logged for a while. try reX in ipa if the product gets dirty
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