Synthesis of Amphetamine from P2NP via SnCl2 and Zn

[Bigballen]

How much desired acid to add at the end?

 

[blacky2340]

Pour 10ml acetone onto 1ml concentrated 97%+ sulfuric acid 10:1 ratio. Use pipette or syringe to drop the solution slowly until pH 5.5 is reached. If overacidified, add more freebase, if way overacidified and turns into liquid then to a/b and recryistalize.

 

[ActionAyi]

I have thought about toulene too but i think the difference of density is too low isnt it ?

 

[sandman]

I don't think this works. I hope it does and will have to try it.

 

[TucoSalamanca.]

I hope you succeed, mate, I failed.

 

[TucoSalamanca.]

Have you done this method

 

[mithyl2]

I've done the borohydride method many times with no success. the closest i came was making about 0.2% yield of amphetamine. it was real though. i need this to work very badly, and it's driving me absolutely mad. let us know how the dcm goes.

 

[TucoSalamanca.]

I will write, my friend, do not miss your prayers so that this synthesis can be realised, thank you.

 

[TucoSalamanca.]

I couldn't synthesise today, I'll do it tomorrow and report back.

 

[ActionAyi]

is there any other way for extract than DCM ?
Maybe n-Hexane ?

 

[August]

Hello friends, does this reaction not just produce phenylethylamine (PEA) or am I just dumb (strong possibility)

 

[Amin. M]

Hello my friend
I read your comment and enjoyed it
How did you get pure amphetamine (in the second step)?
Please advise which method of producing amphetamine is better and ultimately has a higher percentage of purity
And that he procured the raw materials through the store
(I don't have a professional laboratory)