How to synthesise 4-MethylProPioPhenone?

[hlebsladky2]

Hello, people! I've come here with such a question since there are tremendous difficulties with getting 4MP appeared recently. I don't want to order it from China or something. I know that the synthesis of 4MP ain't far harder from Bromination (4mmc). So, I want to craft it by myself. I have found Friedel-Crafts reaction lately but it didn't help me much as I didn't find exact info. Does anybody know how to do it? Merci!

 

[Netflix]

You can order it from europe also what problem you see

 

[billian1]

14.8 g (0.1 mol) of 4'-methylpropiophenone are introduced into 100 ml of chloroform, in the presence of a small amount of finely ground aluminium chloride, and a solution of 15.9 g (0.1 mol; 5 ml) of bromine, in 20 ml of chloroform is added dropwise whilst cooling with an ice bath. The mixture is left to react overnight at ambient temperature. It is then filtered, the solvent is evaporated off from the filtrate and the crystalline residue is washed with diethyl ether. 21.5 g of crystals are collected. And if you might need any Forder questions or to order just PM mee mate we only deal with our clients from EU only

 

[hlebsladky2]

Too much of risk. Such post shippings are dangerous in my country.

 

[billian1]

Nope not dangerous when it concerns us sir just PM and I'll give you directions on how things work discreetly Okey