After the first trials of P2NP, ( https://bbzzzsvqcrqtki6umym6itiixfhn...d-help-for-a-p2np-method-first-try-pics.1316/ )
finally the following
for this first time, the idea is to respect each step of the video ( https://bbzzzsvqcrqtki6umym6itiixfhn...of-amphetamine-from-p2np-via-al-hg-video.196/ )
I was very attentive, so I don't have time to take lots of photos, just a few
- Cutting of aluminum strips and then into "small squares". I put them in an electric coffee grinder and I "push" 12x. It was long and boring.
note: for the first test I simply took an old first price aluminum roll that was lying around...
- 10gr P2NP + 100ml isopropanol + 50ml glacial acetic acid were heated until dissolved and set aside
- 50gr of caustic soda + 150ml H2O have been prepared and bottled in the fridge.
- 2gr of mercury with 20ml of 60% nitric acid, I didn't dare to stir too regularly because of the fumes, so it took longer than on the video.
30 or 40 minutes in all to obtain a clear yellow mercury nitrate liquid. I put this in an amber vial in the fridge.
- 5ml of mercury nitrate were added to the aluminum and 1L H2O, I mixed regularly..., the water became cloudy, then gray, the aluminum began to float.
but I let it continue, I wanted it to stop bubbling.... but almost all the aluminum melted, it never stopped.... I threw it all away.
- I start again, 5ml of nitrate of mercury were added to the aluminum and 1L H2O, I mixed regularly..., the water became cloudy, then grey, the aluminum began to float and I started filtering.
- I put my bottle of N2PN in the balloon, it started to smoke even before I had time to put the condenser. it quickly heated up, I cooled it in a water bath with a few ice cubes but a few drops squirted out of the top of the condenser then it calmed down...
I put in the water, pull him back, try to coax him.. mixed... put it back in the water a bit when it swelled, then it started to bubble but stop swelling, I left it like that for a while, until until it stops making bubbles... we would have it that a little cement was in the mixture...
- I filtered the mixture and added my caustic soda mixture
- after more or less 20min I had 2 coats, the upper one transparent
- I took with a syringe a maximum of this transparent liquid (ph 11) and put in a beaker
- I made a mixture of 20ml of acetone + 2 ml of sulfuric acid
- I had to put + - 13ml in my liquid to get to a ph of 6, a thick pasta is in the liquid
- gravity filtration, it becomes magnificent cream
- drying (still finishing)
A big thank you to all for introducing me to chemistry
finally the following
for this first time, the idea is to respect each step of the video ( https://bbzzzsvqcrqtki6umym6itiixfhn...of-amphetamine-from-p2np-via-al-hg-video.196/ )
I was very attentive, so I don't have time to take lots of photos, just a few
- Cutting of aluminum strips and then into "small squares". I put them in an electric coffee grinder and I "push" 12x. It was long and boring.
note: for the first test I simply took an old first price aluminum roll that was lying around...
- 10gr P2NP + 100ml isopropanol + 50ml glacial acetic acid were heated until dissolved and set aside
- 50gr of caustic soda + 150ml H2O have been prepared and bottled in the fridge.
- 2gr of mercury with 20ml of 60% nitric acid, I didn't dare to stir too regularly because of the fumes, so it took longer than on the video.
30 or 40 minutes in all to obtain a clear yellow mercury nitrate liquid. I put this in an amber vial in the fridge.
- 5ml of mercury nitrate were added to the aluminum and 1L H2O, I mixed regularly..., the water became cloudy, then gray, the aluminum began to float.
but I let it continue, I wanted it to stop bubbling.... but almost all the aluminum melted, it never stopped.... I threw it all away.
- I start again, 5ml of nitrate of mercury were added to the aluminum and 1L H2O, I mixed regularly..., the water became cloudy, then grey, the aluminum began to float and I started filtering.
- I put my bottle of N2PN in the balloon, it started to smoke even before I had time to put the condenser. it quickly heated up, I cooled it in a water bath with a few ice cubes but a few drops squirted out of the top of the condenser then it calmed down...
I put in the water, pull him back, try to coax him.. mixed... put it back in the water a bit when it swelled, then it started to bubble but stop swelling, I left it like that for a while, until until it stops making bubbles... we would have it that a little cement was in the mixture...
- I filtered the mixture and added my caustic soda mixture
- after more or less 20min I had 2 coats, the upper one transparent
- I took with a syringe a maximum of this transparent liquid (ph 11) and put in a beaker
- I made a mixture of 20ml of acetone + 2 ml of sulfuric acid
- I had to put + - 13ml in my liquid to get to a ph of 6, a thick pasta is in the liquid
- gravity filtration, it becomes magnificent cream
- drying (still finishing)
A big thank you to all for introducing me to chemistry
