synthesis

Introduction Methoxetamine (also known as MXE, 3-MeO-2-Oxo-PCE, 2-(ethylamino)-2-(3-methoxyphenyl)cyclohexan-1-one) is an arylcyclohexylamine and a derivative of eticyclidine (PCE). It can also be thought of as the β-Keto-derivative of 3-methoxyeticyclidine (3-MeO-PCE), or the N-ethyl homologue...

Introduction The procedure below describes the oxidation of benzyl alcohol to benzaldehyde in high yield using aqueous nitric acid as an oxidizer. Other methods of oxidizing benzyl alcohol to benzaldehyde are well-known, including those using chlorochromates, persulfate, or activated manganese...

Reactions with Grignard Reagents. A Grignard reagent has a formula RMgX where X is a halogen, and R is an alkyl or aryl (based on a benzene ring) group. For the purposes of this topic, we shall take R to be an alkyl group (e.g., BuMgBr). Grignard reagents are made by adding the halogenoalkane to...

Introduction This topic is represented alpha-PVP synthesis way in a medium scale 1-10 kg. There are elaborated video tutorials, which are allowed to produce this substance to anybody. Also, you can find here a list of necessary equipment and reagents. Equipment and glassware: Round bottom...