amphetamine and p2np Tin(II) Chloride
I want to synthesize with . How can I do the Nabh4 method? I want to do it with 10gr p2np. Can you write all the details for the test?
From sodium ethyl sulfate and a metal nitrite.
1,5 mol sodyum nitrit (103,5 g), 1 mol sodyum etil sülfat (158 g) ve 0,0625 mol K2C03 (8,6 g) ile iyice karıştırılır. Karışım daha sonra 125-130 °C'ye ısıtılır; bu sıcaklıkta nitroetan oluşur oluşmaz damıtılır. Distilasyon akışı önemli ölçüde...
I'm distilling 103.5 grams of sodium nitrite, 158 grams of sodium ethyl sulfate and 8.6 grams of potassium carbonate and it's not distilling, it's a really bad problem. During the reaction it turns into stone and is very difficult to clean, synthesis always fails.
Preparation of Nitroethane by Gerard Desseigne & Henri Giral
The reaction flask is charged with:26.5 g (0.0625 * 3moles) of tech grade K2CO3 dissolved in 137 g of water320 g of 97% tech sodium nitrite
6 ml of cetyl-oleic alcohol or oleic alcoholm(antifoaming agent)Vol of the mixture is about 420...
The site you mentioned, Nitrochemis, says it only ships to the European Union. Can it be sent to Turkey because Türkiye is not a member of the European Union?
Ammonium Acetate Catalysis in Excess Nitroethane3
A solution of benzaldehyde (6.4 g) and ammonium acetate (1.0 g) in nitroethane (20 mL) was heated to reflux for 5 h. On cooling, after removal of the solvent, the residue was purified by column chromatography on silica gel 60 N (neutral...