2-(4-hydroxy-3-methoxy-phenyl)-nitroethene/Vanillin nitrostyrene
The nitrosyrene resulting from condensation of vanillin (4-hydroxy-3-methoxy-benzaldehyde) It synthesizes this. It is possible to synthesize mda with this reagent. How can I do this?
https://www.sciencemadness.org/talk/viewthread.php?tid=30506
I think there is such a topic, is this a reagent precursor for mda, can I synthesize it and synthesize mda?
1gr p2np
3.5ml acetone
2.94gr tin registered
10ml cold water 0.28ml hcl
14ml h2o 14gr no
3.5ml dcm
4.2ml glacial acetic acid
0.7gr
7ml h2o 3.5gr no
3.5ml dcm 3x1.4ml dcm
3.5ml acetone desired acid
I'll do this in my synth tomorrow. There are rumors that ethyl acetate does not oxidize, let's see...
Let me tell you how to do it, first I will add 10ml ipa 80ml h2o, then I will add 3.5gr nabh4, then I will add 2gr p2np, not exceeding 60 degrees, then I will dissolve copper chloride 456mg in 1ml water and add it, not exceeding 80 degrees, then I will heat it to 80 degrees for 30 minutes, I...
How many ml of copper chloride 200mg will I dissolve in water and add 1ml? First I add ipa and water, then I add nabh4, then I add p2np so that it does not exceed 60 degrees, the temperature increases, but when I add copper chloride 200mg, the temperature does not increase, I dissolve it in 5ml...