Next step
Take
2-bromo-4methylopropiophenone 100g\50ml in dcm 500ml= 550ml
And monomethyloamine 40 in water 200ml
And take biger jar 750ml
drop 2b4m in dcm to big jar
and later monomethyloamine
use bag and tabe and shake 30 min
the production of a few grams and a few kg is a big difference. In my opinion, xylene or dcm is the best for pare kg production, when the entire synthesis when working with the reactor takes 12 hours. every step must be well done, best try small amounts from 100g and then try after some time...
Chemicals
{100g}
2-bromo-4methylopropiophenone
{500ml} dcm toulen or benzen
{200ml} methyloamine 40% in water
{3x300ml} cheap water from shop with no gas!!!
{500ml} acetone technical from the construction shop
{55ml} acid hcl 35%-38% if you have 31% acid then we need more to use
This all what we...
Yes you can use dcm toulen or benzen
You need to made
~2xJar
~1xTape
~2xPlastic Bag
~1xFunnel
~2xSyringe 100ml \ 50ml
~Old t~shirt
Whis is what you need form
Yes you can use dcm toulen or benzen
You need to made
~2xJar
~1xTape
~2xPlastic Bag
~1xFunnel
~2xSyringe 100ml \ 50ml
~Old t~shirt
Whis is what you need form equipment:)
2 times washing water alone is not enough rinsing should be from 3 to 5 water must not be empty at the end and why water and hydrochloric acid then need a lot of smearing too much work and smells