don't use toluene, it is not working at all .
I think steam destination is the best.
my black liquid transfer to a light yellow liquid.
but it takes a long time, and my first try was not so good.
I had only a little from 100ml black liquid.
my next try I use a 3 neck flask, I connect my pear...
Poland to Europe, no problem at all . if you can choose shipping company, use one that is active in Poland and in your country. then you are even more safe.
people say that the free base can be extract with dcm or by using steam destilation .
if I choose for the second one do I need first add water to the substance ?
how do you prepaire your NaOH solution with water or methanol ?
I also ask before if I add the NaOH solution to the N-formy if I must boil it again, and they say no
Because the temp be not higher than 60°c
To me, this makes no sense, but this is what people say here.
I personally think these...
yesterday I prepared a solution off 300ml methanol + 35gr NaOH it takes 3 hours to solve, but I think this is allot better this way
Because we need methanol anyway in an later stadium . and then you are sure there is no water left in the solution.
but I think you still need HCl to boil with...
I read someware some months ago, users who ask questions about it
and I remember if the bubbling stops it is ready, but I don't know in what context it was placed
this makes no sense at al after we got ph14 if you add than acid again your ph drops back to 1 also if we add methanol ph drops again
@HIGGS BOSSON @G.Patton
@Yusuf
sorry edit not possible
I did not know that basified what possible with NaOH+methanol ?
so what you are saying is that after you cook your N-formy with HCl for two hours, you're basified with NaOH+methanol ?
don't get this ???
hello
I read many times on the forum people that ask about bubbles in amphetamine production
they ask how long the bubbles last.
I search for weeks but can not find where those questions were ask.
I need to know because I need those bubbles in my syntheses to
today I try again.
after boiling with HCl for two hours, I separate layers.
keep the black layer and basified to ph14 keep it mix for an hour .
then leth it rest for 6 hours and remove the water layer .
after this I add toluene to the black layer but no layers form
and product destroyed...
hello,
after boiling N-formy with HCL for two hours, do we first need to separate it
before we bring it to ph14 ?
and when we add the NaOH, do we need to boil the solution again before washing with toluene ?
Thank you