mda

  1. Irving Langmuir

    [OTC] Synthesis of MDA from helional

    The aim of this post is to summarize several months of research and testing. It would be great if everyone could share their results and their thoughts in order to perfect this synthesis route. All the reagents I'll be using can probably be found in any hardware store, except for helional...
  2. fidelis

    carbamate route to mda/mdma

    haiii i havent seen this posted here yet. i stole it from the vespiary, so heres the original thread :3 (i added numbers to make things easier, lmk if i need to fix anything) There are some very promising, unexplored synthesis routes from alpha-methyl-3,4-methylenedioxypheny-propionamide to...
  3. M

    Piperonal to Isasfrol

    Question 
    Hello, swim have Piperonal but no nitromethane so is ist Possible to reduce piperonal to Isosafrol just simple like fe/hcl? And the other question how can i make formamid from Urea (like Adblue)? Thank you have a nice day
  4. P

    Theoretical investigation: Baylis-Hillman PEA synthesis via Oxazolidone/Oxazolone intermediates

    Introduction: A certain vendor online (that shall not be named) appears to be suggesting a "novel" route to phenethylamines. The reaction from aldehyde to amine occurs in 3 distinct steps: 1) A Baylis-Hillman reaction is first used to couple an aryl aldehyde with acrylamide using a tertiary...
  5. T

    MDP2P FROM PIPERONAL

    Question 
    in the synthesis of piperonal and nitroethane, Could I replace it with nitromethane?
  6. C

    DMSO method

    Question 
    I was reading the 1st edition of "Advanced Techniques of Clandestine Psychedelic & Amphetamine Manufacture" and I got to the chapter 16 which explains a rather simple method using dimethylsulfoxide, conc. sulfuric acid and NaBr/KBr to obtain bromosafrole in order to synthetize MDA/MDMA Has...
  7. C

    MDA synthesis reccomendation

    Question 
    Greetings, fellow underground chemists I am looking for a reccomendation on how to make MDA from M.D.phenylacetone and ammonium formate Anybody knows a process to obtain a good yield without the use of chlorine gas? Should I follow one of the processes explained on the website? If yes, which...
  8. P

    MDA synth

    MDA Hi! One could be looking for advices for synthesizing MDA from PMK. PMK- ethyl glyc. -> PMK Q1) Could/should one vacuum distill PMK to purify? Anyone knows PMK distill temp at vacuum pump level vacuum? Then reductive amination of PMK with anhydrous ammonia and hydrogen in presence of...
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