1-naphthoyl chloride

  1. WillD

    JWH-018 synthesis

    Reaction scheme: Equipment and glassware: 50 L Batch reactor, which is equipped with drip funnel, top stirrer, thermometer, temperature control system (cooling) and reflux condenser; 10 L Flask; Retort stand and clamp for securing apparatus (optional); Reflux condenser; Top stirrer; Heating...
  2. WillD

    3-(1-Naphthoyl)indole Synthesis

    Reagents: Indole (cas 120-72-9) 1000 g; Dichloromethane (CH2Cl2) 15 l; Tin(IV) chloride (SnCl4) 2000 ml; 1-Naphthoyl chloride (cas 879-18-5) 1627 g; Nitromethane (cas 75-52-5) 10 l; Distilled water 20 l; Ethyl acetate (EtOAc) 15 l; Sodium or magnesium sulphate (Na2SO4 or MgSO4); Equipment and...
  3. WillD

    JWH-018 synthesis. Small scale.

    Reaction scheme: Reagents: Indole (cas 120-72-9) 0.117 g; Aluminum oxide (Al2O3) 1 g; 1-Naphthoyl chloride (cas 879-18-5) 0.286 g; Sodium carbonate (Na2CO3) 0.16 g; 1-Bromopentane (cas 110-53-2) 0.18 g; Ethanol (EtOH) 60 ml; Distilled water; Equipment and glassware: Microwave vial 5 ml...
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