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ok, I will publish my synthesis here for revision and advice. step 4 changed: diphenylacetonitrile (50 g), 1-dimethylamino-2-chloropropane hydrochloride (50 g)(think can use any 1-dimethylamino-2-halopropane), 50% sodium hydroxide solution (80 g), water (40 ml), toluene (125 ml) and...

step 1: can change benzene to xylene as solvent? step 3: can change thionyl chloride to some bromine, TBAB f.e.?

what about path with 1,1-diphenylbutane-2-sulfonic acid as precursor?

What method for recrystallizing? Need DCM or EtOH for solvent?

did you use ice or dcm extraction, tried this writeup for mdmb-5br-inaca, stir 4h at 80C, but there isnt powder in ice water, only some oil

What will come of the synthesis of this inca and pentane?

there is writeup from seller, main raw is mdmb-5br-inaca. its safe mix all at once? 3 hour of mix enough? after reaction possible add only a lot of cold brine and wait crystalization without dcm/ethanol/fridge?

hi guys, have some dmf, mdmb-inaca, 5-bromo-1-pentene and potassium carbonate. need practical workup for cooking. thx