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I did TLC, after 3 hours conversion almost 100%, 4hours no precursor presented (ideally do 3-4 hours, but 2-3 hours is usually fine too)

Not necessary

Another question I have - is 2-3 hours stirring & heating sufficient to drive this reaction to completion, or should I go with 4-5 hours like mentioned in some other write-ups?

Congrats bro! Were you able to get solid product in the end or was it still oily? Also would you mind providing the full write-up for the synthesis you followed if you have?

Hi all u beautiful souls of bbgate :-) I have some information along with questions pertaining to the synthesis of MDMB-4en-PINACA // Methyl 3,3-dimethyl-2-(1-(pent-4-en-1-yl)-1H-indazole-3-carboxamido)butanoate // C20H27N3O3 // Cas no. 2504100-70-1 (also colloquially & incorrectly known as...