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about 45-60% from 2,5 dmba the only problem is that its needs to run at very cold conditions (about 0oC) i run it inside a freezer but ice salt bath will do , i run it at about 10oC and the 2ch comes out dark and i know it supposed to be light yellow , you can see in the IPA second pic on the...

sorry for bad english ill try to be more clear , i meant chunks , the photo where there are 2cb chunks floating , i took one of them a dropped them into a clean toluene and added hcl and salt was generated , so i guess that the toluene that used for extraction carrys with it stuff that doesn't...

didnt had a chance to check i dont think i can get elemental bromine since you need special approval but ill ask maybe in small quantity , i know for a fact that my friend in other country was successful with the synthesis 100% so its just me doing something wrong , he told with that i need to...

edit : i've took a chunk that floated after the addition of NAOH which makes 2cb not soluble in water and dropped it into a clean toluene and added hcl and it did generate white salt , my guess is there are other stuff in the toluene that prevent the salt from generating , so i thought of an...

hey i oppened a new threat with the process i hope you can help me https://chemforum.info/index.php?threads/novel-2cb-synthesis-problems-with-pictures-please-help-me-to-figure-it-out.1560/ i hope you can help me there , also i have acess to DCM ' and what do you think about the reduction...

i've come around this novel way and tried to do it , but run into problems i hope you can help me figure it out. i've ordered 1kg of 2,5 Dmba from china. this is the steps : 1. Dissolve 8.3g (50mmol) 2,5-Dimethoxy Benzaldehyde in 50ml Methanol and 6.1g(100mmol) Nitromethane in 1L beaker. Stir...

i have a loot of goo now , i added 35% hcl to toluene and it supposed to generate 2CB hcl salt , but it doesnt form , ill check with my chemical supplier tomorrow about DCM , any idea why salt doesnt from ? , if i add hcl to toluene with 2cb it will sink as dark oil?

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i was trying to make 2cb this days , at the last stage after bromination , i add NAOH to make 2cb go to the toluene layer (that added a bit later) , the toluene is sucked out and supposed to generate 2cbHCL when adding hcl , but instead only a black goo is generated that sinks at the bottom , i...

i saw a micro scale for MXE , and ketamine , but any other ones? o-pce , 3 ho p***** . p***** etc?

hey i opened a con' with you , waiting for a reply from you :)

I saw listings on 4mp here and also on alibaba , but not on 2br4mp which comes as a powder and not liquid. I saw few listings of chinese companys https://wap.guidechem.com/cas/1451-82-7.html Didnt check about the legitness of the companys , but giving the opertunity , isnt it better to order...

I want to order tryptamine from china , the only thing is i am not sure how stable it is ? It should be kept at a cool place away from the atmosphere (vaccum sealed) I worry that it will degrade in transportation (20 days?) I searched for some one that ships it in hcl form with not much luck...