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  1. C

    Video instructions.

    Hello Heisenberg I respect & appreciate what you are doing. I have some questions which I hope you might help me with answers. My questions are 1. Will non resolved meth crystallize 2. Does non resolved meth crystals itch or choke the throat when smoked A friend got some meth oil not sure...
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    Resolution

    Hello tovenaar, Kindly share how to perform Methamphetamine resolution the Mexican way with me pls.
  3. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    So heat is applied to boil off excess solvent then allowed to cool for crystallization to occur. Do you think one can proceed to Baeyer villager reaction without crystallization MPB?
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    Anyone ever try the Bayer-villager route to P2P?

    I need help with this reaction. I can’t even go past the first step of obtaining MPB crystals. I would like to obtain the MPB crystal without performing the vacuum distillation. I gas my MEK + Benzaldehyde, allow it sit for 48hrs then I decant bottom layer. Brown layer is washed with water &...
  5. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    William D. Can you pls pls explain the procedure of getting MPB crystal without doing the vacuum distillation. I have followed the steps suggested but it seems I can’t get it right. I have washed, I have neutralized, I have dissolved in ethanol and I have frozen but for some reason I don’t know...
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    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    My crystal liquifies at room temperature, how do I solve this problem
  7. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    How do you get the MPB to solidify? In the freezer i see the crystals but outside the freezer it liquifies.
  8. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    When you say u wouldn’t titrate any more does it mean no more hydroxide wash after the MEK + Benzaldehyde reaction. Will it result in more quantities of MPB?
  9. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    I already have the MPB solution and would like to get the crystals without distillation. The adol condensation was done through acid gassing. Do you think if acid is introduced in the Benz + MEK solution through gassing and heated up to 90-110°C for 3-5 hrs and washed with hcl before adding 10%...
  10. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    I already have the MPB solution and would like to get the crystals without distillation. The adol condensation was done through acid gassing. Do you think if acid is introduced in the Benz + MEK solution through gassing and heated up to 90-110°C for 3-5 hrs and washed with hcl before adding 10%...
  11. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    Do you cool the BENZ & MEK mixture before adding the 10% KoH solution. With this procedure there will be no need for vacuum distillation right.
  12. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    Kindly share the procedure of obtaining MPB oil from crude mixture if you don’t want to vacuum distill.
  13. C

    Phenylacetone (P2P) synthesis from benzaldehyde with butanone

    Is the alkaline wash of MPB necessary? I noticed you didn’t do that but distilled after the water wash
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