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I realized I did it wrong p2p-> nform . I didn't let it go for 5 hours at 150 degrees. after the temperature rises to 150 degrees (for me it takes about ~4 hours. when it reaches 150 degrees, it has to be kept there for 6 hours and I got 8L of nform, 10L of P2P. I take 2L of nform from a...

good afternoon ! I really like this synthesis, I've made it several times. but the yield when I need to get nform will be small at that point. I get 5L of nform from 10L of dirty P2P, and 1.5L from the aqueous layer. so in the end, after steam distillation, instead of 8.5 L yield, I always...