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I see I did bad assumption thinking that steam distilled freebase will separate from water itself :-/ I combined the brine I had left with NaOH from reaction slury extract and I extracted it with IPA getting a little more of freebase. The puny amount, I think, but, as Albert Hoffman said...

Dear Colleagues. I've read that some of you purify meth freebase by steam distillation. I do not have enough efficient vacuum pump to keep water boiling poing below 60 deg.C so I thought I can instead wash it several times with distilled water. To my surprise...first try of washing created...