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Belfort, thanks. I will try your suggestion out.

G.Patton, Gordon Ramsey or any chemist in this community - can you offer any solutions to this problem? Any help is greatly appreciated. Thanks in advance.

Btcboss2022 Thank you for the reply to my post. The powder came in wrapped thick plastic bag in a cardboard box as usual. I only received it 1.5months ago but how long in storage before me, who knows. I store it in a cool room temp space. I did 2 reactions in total, 1 reaction from 1 box and...

Belfort, thats correct reaction with HCL.

Btcboss2022, please help I followed your recipe for synthesis of pmk 28578-16-7 powder to mdp2p and after refluxing oil separation occur but there was still some white cloudy stuff in the oil and as the oil cooled the white cloudy stuff became thicker like soggy cereal and left me with very...