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  1. Z

    2bromo4 suppliers

    Shitty bromometone = shitty 4mmc :-) you can order on this forum free sample, if you want can recommend you some seller. Just use Heisenberg advices and you will succes with this problem.
  2. Z

    2bromo4methylpropiophenone problem.

    Hello curiousbob221, 2bromo4methylpropiophenone is not disolving in water well, 4methylpropiophenone which is precursor of it also do not dissolve in water - In my opinion it is some alkali residue after cleaning this bromoketone. If it is big quantity that you have ordered, maybe you are able...
  3. Z

    2-bromo-4-chloropropiohenone synthesis. (HBr/H2O2 ?)

    I found an instruction for synthesis 2-bromo-4-chloropropiohenone: "A solution of 15.9 g (0.1 mol) of bromine in 20 ml of chloroform is added dropwise to a solution of 16.8 g (0.1 mol) of 4'-chloropropiophenone in 100 ml of chloroform, in the presence of a small amount of aluminium chloride...
  4. Z

    4′-Methylpropiophenone bromination to 2-bromo-4'-methylpropiophenone. Large scale.

    Which solvent is best for recrystallization 2-bromo-4'-methylpropiophenone? I have tried this method but my 2b4mpp is a little bit dirty - white instead of colorless cristal.
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