I learned the basic synthesis in DCM and I was curios how the cold one is done and it s nothing on the forum about that. It would be great if some expert could help with that
How 4mmc cold synthesis is done?
- Thread starter abis777
- Start date
The reaction time is very short, no more than two hours. The reaction itself is exothermic.
I think there is no point or possibility to even try to do this.
It is devoid of any logic
I think there is no point or possibility to even try to do this.
It is devoid of any logic
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- By PersonVPN
If you make 300-500 g, and do it in DMSO and similar solvents, then yes, of course! The reaction time is 15 minutes.
But if you increase the amount of reagents loaded at least tenfold, then I'm afraid you won't have enough 15 minutes to load all the reagents, to have time to cool the RM, and not to overheat the RM.
Now let's fantasize a little!
Imagine that you load 25 kg of BK4 into a certain vessel....
I'm afraid that at the very least you won't be able to fit it into your crystal washing device, and there can be no talk of stabilizing the reaction process!
So I can only wish you success in your kitchen, with your plastic products.
But if you increase the amount of reagents loaded at least tenfold, then I'm afraid you won't have enough 15 minutes to load all the reagents, to have time to cool the RM, and not to overheat the RM.
Now let's fantasize a little!
Imagine that you load 25 kg of BK4 into a certain vessel....
I'm afraid that at the very least you won't be able to fit it into your crystal washing device, and there can be no talk of stabilizing the reaction process!
So I can only wish you success in your kitchen, with your plastic products.