Question MDP2NP to MDMA, is It's possible?

[jjtr813]

HI,
I have 1-(3,4-Methylenedioxyphenyl)-2-nitroprop-1-ene and LAH.

I know there's a 100 MDA Shulgin route.

Thanks

 

[HerrHaber]

It's just not the most efficient way... even though possible, I would personally enjoy the MDA since significant losses are to be expected at the final monomethylation step. MDP2NP can also be converted to MDP2P and then subjected to reductive amination with methylamine but I have no idea about the convenience of this method as the ketone is pretty sensitive and must be stored in the freezer for the shortest time possible.

 

[loadingST]

I have always wondered how you guys get piperonal, maybe piperonil alcohol ozonolisis who knows, if anyone put piperonal to buy i woud take some even foe the smell ha

 

[CCL4 huffer]

just do a ozonolysis on piperine witch u can extract from blackpeppers if u got the time or just buy as pepper extract.
i think there was also a way to go from vanillin to protocatechuic aldehyde and then piperonal.

 

[loadingST]

There is pmk glycidate my frend but i just mentioned i coud buy piperonal if it was acessabill

 

[CCL4 huffer]

i know u asked how u can get it and i aswered ur question fin.

 

[The-Hive]

acetic acid, urotropine, piperonyl chloride get about 30g piperonal with the purity of 96%